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Author Profile
Raffaele Bellini
M.D. Anderson
Articles by Raffaele Bellini
Effective Reducing Agent From Sigma Aldrich
July 23, 2023
This product was used to reduce ester to aldehydes avoiding the risk to get the corresponding alcohol
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Trifluoroacetic Acid for Boc Deprotection From Oakwood Chemical
July 23, 2023
The goal of the work was to remove the Boc protective group from an amide to go further in the synthesis, following a coupling ...
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Trifluoroacetic Acid From Thermo Scientific For Boc Deprotection
July 23, 2023
We need to deprotect a Boc amine to be able then to link it to a carboxylic acid and form a new peptide bond.
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Di-tert-butyl dicarbonate for Boc Protection
July 23, 2023
The aim was to protect just one side of a diamine to be subsequently able to link it to a second scaffold.
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Synthesis of Schiff Base
July 23, 2023
We synthesized a Schiff base using an amine and an aldehyde. This product will be then linked to a larger scaffold exploiting the ...
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Acid Catalyzed Reaction with Titanium (III) Chloride
June 01, 2023
We tried to get a intramolecular cyclization using TiCl3 as catalyst. Its purpose was to activate the carboxylic functional moiety...
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Bulky Base Works Well for Deprotonation
May 12, 2023
Synthesis of new peptide bond starting from an acyl chloride and an amide in a dry atmosphere of N2, using bulky base.
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Hygroscopic Methanol-d4 for NMR Spectra
May 12, 2023
At the end of a synthesis of a compound, you need to check if the reaction has gone to the right way or not. Several method can be...
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Deprotonation of Mild Acid Protons with Butyllithium
May 09, 2023
The product has been used to deprotonate protons with high pKa that are not possible to deprotonate with more mild bases.
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Ester Reduction with Methyl 4-Bromophenylacetate
May 09, 2023
The corresponding aldehyde will be used to form a bicycle, where the aldehydic moiety will react to form part of the ring ...
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Synthesizing New Peptide Bond with Acryloyl Chloride
May 04, 2023
Synthesis of new peptide bond starting from acyl chloride and an amine. I used 1 equivalent added at 0 °C and then brought to room...
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Chloroform-d Works Well for NMR Spectra
April 25, 2023
After the end of any reaction, there are several methods that can be used to check if it is gone to the right way or not. One of...
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Effective Tetrahydrofuran for Dry Synthesis
April 25, 2023
I used the THF extra dry at a C=0.5 M for the dehydrogenation of a secondary amide. The reaction worked fast, It needed 30 minutes...
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Product Review
Excellent Astrocyte Labeling with Low Background in Mouse Hippocampus
Ksenia Novototskaya
(2)
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We used this antibody to immunofluorescently label astrocytes in the mouse dorsal hippocampus following astrocyte-specific MOR knockdown. The signal was bright,...
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