Acid Catalyzed Reaction with Titanium (III) Chloride

M.D. Anderson

Overall

Quality of Results

Ease-of-Optimization

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Company:

Sigma Aldrich

Product Name:

Titanium (III) Chloride

Catalog Number:

14010

We tried to get a intramolecular cyclization using TiCl3 as catalyst. Its purpose was to activate the carboxylic functional moiety of the structure.

Experimental Design and Results Summary

Application

Catalyst

Starting Material

N/A

Tips

Corrosive

Results Summary

We the aid of the Titanium, we could decrease the energy of the transition state to reach the cyclo-cheton structure. Equivalents = 4.5. Needed to be added dropwise.

DOI or PMID #

N/A

Image Gallery

Summary

The Good

Works well, stable for long periods.

The Bad

Corrosive

The Bottom Line

I would suggest its use for anyone who needs to activate a carboxylic or carbonyl moiety.

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